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11.
Kumita T Sagawa H Auchincloss P Blanis D Bodek A Budd H Eno S Fry CA Harada H Ho YH Kim YK Mori T Olsen SL Shaw NM Sill A Thorndike EH Ueno K Zheng HW Abe K Fujii Y Higashi Y Kim SK Kurihara Y Maki A Nozaki T Omori T Sakai Y Sugimoto Y Takaiwa Y Terada S Walker R Imlay R Kirk P Lim J McNeil RR Metcalf W Myung SS Cheng CP Gu P Li J Li YK Ye MH Zhu YC Abashian A Gotow K Hu KP Low EH Mattson ME Piilonen L Sterner KL Lusin S Rosenfeld C Wang AT Wilson S Frautschi M Kagan H Kass R Trahern CG 《Physical review D: Particles and fields》1990,42(5):1339-1349
12.
Kim YK Auchincloss P Blanis D Bodek A Budd H Eno S Fry CA Harada H Ho YH Kumita T Mori T Olsen SL Shaw NM Sill A Thorndike EH Ueno K Zheng HW Imlay R Kirk P Lim J McNeil RR Metcalf W Myung SS Cheng CP Gu P Li J Li YK Mao ZP Xu YT Zhu YC Abashian A Gotow K Hu KP Low EH Mattson ME Piilonen L Sterner KL Lusin S Rosenfeld C Wang AT Wilson S Frautschi M Kagan H Kass R Trahern CG Breedon RE Kim GN Ko W Lander RL Maeshima K Malchow RL Smith JR Stuart D Williams MC Abe K Fujii Y Higashi Y Kim SK 《Physical review letters》1989,63(17):1772-1775
13.
Eno S Auchincloss P Blanis D Bodek A Budd H Fry CA Harada H Ho YH Kim YK Kumita T Mori T Olsen SL Shaw NM Sill A Thorndike EH Ueno K Zheng HW Imlay R Kirk P Lim J McNeil RR Metcalf W Myung SS Cheng CP Gu P Li J Li YK Mao ZP Xu YT Zhu YC Abashian A Gotow K Hu KP Low EH Mattson ME Piilonen L Sterner KL Lusin S Rosenfeld C Wang AT Wilson S Frautschi M Kagan H Kass R Trahern CG Breedon RE Kim GN Ko W Lander RL Maeshima K Malchow RL Smith JR Stuart D Williams MC Abe K Fujii Y Higashi Y Kim SK 《Physical review letters》1989,63(18):1910-1913
14.
Shaw NM Blanis D Bodek A Budd H Coombes R Eno S Fry CA Harada H Ho YH Kim YK Kumita T Mori T Olsen SL Sill A Thorndike EH Ueno K Zheng HW Imlay R Kirk P Lim J McNeil RR Metcalf W Myung SS Cheng CP Gu P Li J Li YK Mao ZP Xu YT Zhu YC Abashian A Gotow K Hu K Low EH Mattson ME Naito F Piilonen L Sterner KL Lusin S Rosenfeld C Wang AT Wilson S Frautschi M Kagan H Kass R Trahern CG Breedon RE Kim GN Ko W Lander RL Maeshima K Malchow RL Smith JR Sparks K Williams MC Abe K Fujii Y Higashi Y Kim SK 《Physical review letters》1989,63(13):1342-1345
15.
Applications of chalcogenide glass optical fibers 总被引:2,自引:0,他引:2
Chalcogenide-glass fibers based on sulfide, selenide, telluride and their rare-earth-doped compositions are being actively pursued worldwide. Great strides have been made in reducing optical losses using improved chemical purification techniques, but further improvements are needed in both purification and fiberization technology to attain the theoretical optical losses. Despite this, chalcogenide-glass fibers are enabling numerous applications that include laser power delivery, chemical sensing, and imaging, scanning near field microscopy/spectroscopy, IR sources/lasers, amplifiers and optical switches. 相似文献
16.
John T. Shaw Christine E. Brotherton Robert W. Moon Mark D. Winland Mark D. Anderson Keith S. Kyler 《Journal of heterocyclic chemistry》1980,17(1):11-16
A much improved synthesis of the heretofore difficultly obtainable 2,6-diaminopyrazine (4) was afforded by the low-pressure catalytic hydrogenation (palladium on carbon) of 2,6-diazido-pyrazine (2) ; reaction of 2,6-dichloropyrazine (1) and sodium azide gave 2 in 84% yield. The outcome of the reduction was found to be solvent dependent: 1,2-dimethoxyethane containing aqueous ammonia gave 4 in 83% yield; 1,2-dimethoxyethane alone gave 5-aminotetrazolo[1,5-a]-pyrazine (3) in 26% yield. Additional alternative syntheses of 3 and 4 are described. A number of acyl and azo derivatives of 4 were prepared. Reactions of 2 with dimethyl acetylenedicarboxylate and ethyl acetate (base catalyzed) leading to vic-triazole derivatives are also described. 相似文献
17.
The bulky teratiary phosphines P-t-Bu2Ph and P-t-Bu2-p-tol, provide binuclear ruthenium(I) complexes. An X-ray analysis of [Ru2Cl2(CO)4(P-t-Bu2-p-tol)2] shows the RuCl2Ru bridge to be non-planar and to have an Ru---Ru distance of 2.632Å. 相似文献
18.
J. M. Beiriger R. A. Failor K. V. Marsh G. E. Shaw 《Journal of Radioanalytical and Nuclear Chemistry》1988,123(1):21-37
Following the accident at the nuclear reactor at Chernobyl, in the Soviet Union on April 26, 1986, we performed a variety of measurements to determine the level of the radioactive fallout on the western United States. We used gamma-spectroscopy to analyze air filters from the areas around Lawrence Livermore National Laboratory (LLNL), California, and Barrow and Fairbanks, Alaska. Milk from California and imported vegetables were also analyzed. The levels of the various fission products detected were far below the maximum permissable concentration levels.Work performed under the auspices of the U.S. Department of Energy by the Lawrence Livermore National Laboratory under contract number W-7405-ENG-48. 相似文献
19.
Molecular structures of three emissive annular digold compounds [Au2(dmpm)(dtc)]Cl (dmpm = Me2PCH2PMe2,dtc = S2CNEt2), 1 , [Au2(dppm)(dtc)]PF6, (dppm = Ph2PCH2PPh2),2,and [Au2(dppe)(dtc)]-(PF2) (dppe = Ph2P(CH2)2PPh2), 3, were determined. All three compounds are dimetallacycles having two gold atoms bridged by a dithiolate ligand and a diphosphine ligand, the geometry around each gold atom being almost linear. All the dimetal lacy die rings are slightly distorted from planarity with intramolecular Au-Au distances shorter than 3.0 Å. Compound 1 forms a polymeric chain through intermolecular Au-Au contacts (3.061 ? 3.135 Å). Compound 2 forms a tetramer through intermolecular Au-Au interactions (Au-Au distances ranging from 3.086 to 3.222 ). Compound 3 is monomeric. All of the compounds luminesce at 77 K in the solid state. Emissions originating from 3LMCT from dtc ligand to Au excited states are assigned. The emission maxima of 1 ? 3 are at 541,535 and 520 nm respectively and are blue shifted as the number of Au-Au interactions is decreased. 相似文献
20.
McClean S Robinson RC Shaw C Smyth WF 《Rapid communications in mass spectrometry : RCM》2002,16(5):346-354
The characterisation of selected indole alkaloids in a quadrupole ion trap mass spectrometer is presented. Fragmentation profiles for tryptamine, 5-hydroxytryptamine (5-HT), N'-methyl 5-hydroxytryptamine (N'-methyl 5-HT), N',N'-dimethyl 5-hydroxytryptamine (bufotenine), N',N',N'-trimethyl 5-hydroxytryptamine (5-HTQ), and N',N'-dimethyl 5-methoxytryptamine (5-MeODMT) are presented with proposed structures given for each product ion observed. Such MS(n) experiments can be used to differentiate the isobaric molecular ions of the compounds 5-HTQ (M(+)) and 5-MeODMT (MH(+)). The quantitative determination of certain indole alkaloids in the skin secretions of the Australian Golden Bell frog, Litoria aurea, by LC/ESI-ion trap MS is also presented. The concentrations of 5-HT, N'-methyl 5-HT and 5-HTQ were found to be 2.68, 0.26 and 0.54 microg per mg of skin secretion, respectively. 相似文献